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Extra resources for Carbohydrate Chemistry: Proven Synthetic Methods, Volume 2
2. Garegg, P. ; Hultberg, H. Carbohydr. Res. 1981, 93, C10–C11. 3. ; Garegg, P. ; Oscarson, S. J. Carbohydr. Chem. 1983, 2, 305–311. 4. ; Mitsunobu, O. Chem. Lett. 1987, 2033–2036. ; Yoakim, C. Can. J. Chem. 1990, 68, 897–902. 6. ; Nokami, J. Carbohydr. Res. 2008, 343, 2675–2679. 7. ; Yoakim, C. Can. J. Chem. 1990, 68, 897–902. 8. DeNinno, M. ; Etienne, J. ; Duplantier, K. C. Tetrahedron Lett. 1995, 36, 669–672. 9. ; Kusumoto, S. Synlett 1996, 1179–1180. 10. -H. Tetrahedron Lett. 1998, 39, 355–358.
Res. 2008, 343, 2675–2679. 7. ; Yoakim, C. Can. J. Chem. 1990, 68, 897–902. 8. DeNinno, M. ; Etienne, J. ; Duplantier, K. C. Tetrahedron Lett. 1995, 36, 669–672. 9. ; Kusumoto, S. Synlett 1996, 1179–1180. 10. -H. Tetrahedron Lett. 1998, 39, 355–358. 11. ; Reddy, Y. ; Reddy, C. R. Chem. Lett. 1998, 1273–1274. 12. ; Dulina, R. ; Sofia, M. J. J. Org. Chem. 2000, 65, 8387–8390. 13. ; Hamana, H. Tetrahedron Lett. 2000, 41, 5547–5551. 14. Debenham, S. ; Toone, E. J. Tetrahedron: Asymmetry 2000, 11, 385–387.
97 mmol, 91%) as a white foam. 7 (CH3, Ac); HR MALDI-TOF MS: [M + Na]+ calcd. 2149. 14 mmol) was dissolved in dry CH2Cl2 (3 mL) and activated 3Å molecular sieves* (~500 mg) were added. The mixture was stirred for 10 min at rt before cooling to –50°C. ) was added and the mixture was slowly warmed to –30°C over a period of 15 min. 35) was observed. ) in CH2Cl2 (2 mL), which was dried using activated 3Å molecular sieves* (~200 mg), was added dropwise. The resulting * Molecular sieves (Aldrich [St.